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推进剂现代技术 1PDF|Epub|txt|kindle电子书版本网盘下载
- 黄智勇，窦文辉编著 著
- 出版社： 西安：西北工业大学出版社
- ISBN：9787561243350
- 出版时间：2015
- 标注页数：257页
- 文件大小：46MB
- 文件页数：266页
- 主题词：火箭推进剂
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图书目录
PART Ⅰ INSTRUMENTAL ANALYSIS3
CHAPTER 1 GENERALIZATION OF INSTRUMENTAL ANALYSIS3
1.1 GENERALIZATION OF MODERN ANALYTICAL TECHNOLOGY4
1.2 CHARACTERICS OF MODERN ANALYTICAL TECHNOLOGY5
1.3 DEVELOPMENT OF MODERN ANALYTICAL TECHNOLOGY6
CHAPTER 2 GAS CHROMATOGRAPHIC ANALYTICAL TECHNOLOGY8
2.1 GENERALIZATION8
2.2 BASIC PRINCIPLE OF GAS CHROMATOGRAPHY13
2.3 DETERMINATION OF UDMH WITH GAS CHROMATOGRAPHY36
CHAPTER 3 GAS CHROMATOGRPHY-MASS SPECTROSCOPY COMBINATION ANALYTICAL TECHNOLOGY40
3.1 GENERALIZATION40
3.2 BASIC PRINCIPLE OF GAS CHROMATOGRAPHY-MASS SPECTROSCOPY COMBINATION42
3.3 DETERMINATION OF THE OXIDIZED PRODUCT OF UDMH WITH GC-MS57
CHAPTER 4 NEAR INFRARED ANALYTICAL TECHNOLOGY59
4.1 GENERALIZATION59
4.2 BASIC PRINCIPLE OF NIR ANALYSIS61
4.3 DETERMINATION OF THE COMPONENT CONTENT OF NITRIC ACID-27S69
4.4. DETERMINE THE COMPONENT CONTENT OF DT-3 WITH NIR METHOD71
CHAPTER 5 AUTOMATIC COUNTER OF PARTICULATE74
5.1 GENERALIZATION74
5.2 PRINCIPLE OF AUTOMATIC COUNTER OF PARTICULATE74
5.3 DETERMINATION OF PARTICULATE CONTENT IN UDMH WITH AUTOMATIC COUNTER77
PART Ⅱ ASSAY OF UDMH89
CHAPTER 6 INTRODUCTION TO PROPELLANTS89
6.1 CLASSIFICATION OF PROPELLANTS89
6.2 FUNCTION AND CLASSIFICATION OF LIQUID PROPELLANTS90
6.3 THE REQUIREMENTS FOR LIQUID PROPELLANTS94
CHAPTER 7 UDMH'S USE AND MANAGEMENT98
7.1 PHYSICO-CHEMICAL PROPERTIES OF UDMH98
7.2 PRODUCTION AND TECHNICAL SPECIFICATION OF UDMH105
7.3 TOXICITY AND ITS PROTECTION109
7.4 THE DANGER OF FIRING AND EXPLOSION116
7.5 MATERIAL COMPATIBILITY120
7.6 STORAGE,TRANSPORTATION AND TRANFERRING123
7.7 SAMPLING PRINCIPLE FOR UDMH125
7.8 ATTENTIONS FOR SAFETY128
CHAPTER 8 FUNDAMENTALS OF UDMH ASSAY130
8.1 ACID-BASE TITRATION130
8.2 MASS ANALYSIS138
CHAPTER 9 ASSAY OF UDMH142
9.1 TECHNICAL REQUIREMENT AND APPEARANCE INSPECTION142
9.2 THE CONTENT OF UDMH,DIMETHYL AMMONIUM AND UNSYMMETRICAL HYDRAZONE DETERMINATION WITH ACID-BASE TITRATION143
9.3 WATER CONTENT DETERMINATION WITH RAPID GAS MEASUREMENT147
9.4 DETERMINE THE CONTENT OF UDMH,DIMETHYL AMMONIUM AND UNSYMMETRICAL HYDRAZONE WITH GAS CHROMATOGRAPHY152
9.5 DETERMINATION OF THE MECHANICAL IMPURITY CONTENT IN UDMH160
9.6 DETERMINATION OF DENSITY162
APPENDIX 9.1 VERIFICATION OF VOLUMETERIC APPARATUS163
APPENDIX 9.2 COMPOUNDING AND DETERMINATION OF STANDARD SOLUTION IN THE ASSAY OF UDMH166
PART Ⅲ ASSAY OF NITRIC ACID-27S173
CHAPTER 10 USE AND MANAGEMENT OF NITRIC ACID-27S173
10.1 PHYSIC-CHEMICAL PROPERTIES OF NITRIC ACID-27S173
10.2 USE AND MANAGEMENT OF NITRIC ACID-27S176
CHAPTER 11 FUNDAMENTALS FOR THE ASSAY OF NITRIC ACID-27S196
11.1 OXIDATION-REDUCTION TITRATION196
11.2 GRAVIMETRY202
CHAPTER 12 ASSAY OF NITRIC ACID-27S207
12.1 TECHNICAL REQUIREMENTS AND APPEARANCE INSPECTION207
12.2 DENSITY DETERMINATION208
12.3 NITROGEN TETRAOXIDE CONTENT DETERMINATION210
12.4 DETERMINATION OF WATER CONTENT212
12.5 DETERMINATION OF PHOSPHORIC ACID CONTENT215
12.6 DETERMINATION OF HYDROFLUORIC ACID CONTENT218
12.7 DETERMINATION OF THE CONTENT OF BURNED RESIDUE223
APPENDIX 12.1 THE COMPUNDING OF c(1/5 KMnO4)=0.2mol/L STANDARD SOLUTION225
APPENDIX 12.2 COMPOUNDING AND DETERMINATION OF STANDARD SOLUTION IN NITRIC ACID-27S ASSAY226
APPENDIX 12.3 COMPOUNDING OF INDICATORS FOR THE ASSAY OF NITRIC ACID-27S230
APPENDIX 12.4 THE ERROR MATTER IN THE ASSAY OF LIQUID PROPELLANT230
PART Ⅳ ASSAY OF DT-3230
CHAPTER 13 ASSAY OF DT-3243
13.1 COMPOUNDING OF STANDARD SOLUTIONS AND MIXED INDICATORS243
13.2 SAMPLING245
13.3 APPEARANCE INSPECTION246
13.4 COMPONENTS ANALYSIS246
13.5 WATER CONTENT ANALYSIS249
13.6 PARTICLE MATTER DETERMINATION250
13.7 RESIDUE DETERMINATION252
APPENDIX 13.1 CALIBRATION OF PRECISION GLASS MEASURING VESSELS253
APPENDIX 13.2 OPERATION OF ACIDOMETER AND NEUTRALIZITION OF FORMALDEHYDE255
REFERENCE257